I'm quite sure this is the same bug  as Bug #36252 and Bug #111541.

It should be a EJECT command problem (both launched in terminal and via 
Nautilus)
UMOUNT command works fine.

Check out my comments on Bug #36252
https://bugs.launchpad.net/ubuntu/+source/nautilus/+bug/36252/comments/26

and Bug #111541
https://bugs.launchpad.net/ubuntu/+source/eject/+bug/111541/comments/12

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nautilus, media containing multiple partitions cannot be unmounted (USB 
connected)
https://bugs.launchpad.net/bugs/108643
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